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on't buy reviews. Reviews are how Amazon rates your business on the basis of positive reviews. Buying reviews is a short term strategy but can be harmful in the long term. The symmetry of the high temperature phase of HfP2O7 is investigated by Rietveld refinement of neutron diffraction data. Unusual effects in the 51V NMR spectra of HfV2O7 and ZrV2O7 are also reported. Chapter 6 outlines preliminary work on computational methods to investigate the structural dependence of the 31P NMR chemical shift of pyrophosphate materials. The experience was so fun and inspiring that I and others kept going back